HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyaniline → 4-((2-Methoxyphenyl)sulfamoyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyaniline | HCID 7000 | — |
| Reactant | 4-(Chlorosulfonyl)benzoic acid | HCID 82385 | — |
| Product | 4-((2-Methoxyphenyl)sulfamoyl)benzoic acid | HCID 2333505 | 95.7% |
Reaction Steps
Using o-anisidine (0.585 ml, 5.0 mmol) and 4-(chlorosulfonyl)benzoic acid (1.15 g, 5.0 mmol), the procedure of Reference Example 2 was repeated to obtain 1.47 g (95.5%) of the title compound in the form of pink powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-bcfcdbed56674c439cbfcd16edd11134 |
| Source note | uspto-grants-1998_03 |