HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propanal → 3-Carene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propanal | HCID 527 | — |
| Reactant | Oxygen | HCID 977 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Product | 3-Carene | HCID 26049 | — |
Reaction Steps
Δ-3-carene was epoxidized by the above-described procedure, using Di(acetate)3 as catalyst (1% based on the weight of Δ-3-carene) and ethyl acetate as solvent (volume ratio solvent to Δ-3-carene 3:1). The final mol ratio propionaldehyde to Δ-3-carene was 1.5:1, oxygen was bubbled through at a rate of 8 liters/hour, and reaction time was 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04721798 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-9e95533bb7ed49bd91bdefb7a74d85e5 |
| Source note | uspto-grants-1988_01 |