huagongshe.com
HRID2414193

反应详情

EQUATION

反应方程式

HRID 2414193 的结构方程式

REACTANTS

反应物

2
结构：C=CCBr
HCID7841

Allyl bromide

C3H5Br

结构：CS(=O)(=O)N1CCOc2ccc(C3=NNC(=O)CC3)cc21
HCID14230055

未命名化合物

PRODUCTS

生成物

1
结构：C=CCN1N=C(c2ccc3c(c2)N(S(C)(=O)=O)CCO3)CCC1=O
HCID15599406

未命名化合物

PROCEDURE

实验过程

6-(3,4-Dihydro-4-methanesulfonyl-1,4(2H)-benzoxazin-6-yl)-2,3,4,5-tetrahydropyridazin-3-one was reacted with allyl bromide instead of methyl iodide, following the procedure of Example 9. The title compound was recovered, yield 2.03 g, mp 153°-155° C.

WORKUP

后处理

  1. customThe title compound was recovered