HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Sodium;3-phenylprop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Harpagoside | HCID 5281542 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Sodium;3-phenylprop-2-enoate | HCID 517350 | — |
| Product | HCID 44438955 | HCID 44438955 | — |
Reaction Steps
560 mg of harpagoside (LN-1) was dissolved in 20 ml of methanol, mixed with 1 ml of 1N sodium hydroxide, allowed to stand overnight at room temperature and then passed through Sephadex LH-20 (solvent: 80% methanol) column. 400 mg of harpagide and 125 mg of sodium cinnamate were obtained from the eluate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06812214B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-f97b1318897a45fe9030ca9801468f70 |
| Source note | uspto-grants-2004_11 |