HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9976315, compound → Methyl heptanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9976315 | HCID 9976315 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl heptanoate | HCID 7826 | 256% |
Reaction Steps
Palladium on carbon (10 mol %, 5 mg) was added to a solution of alkene 27 (24 mg, 0.065 mmol) in MeOH (2.0 mL). The flask was evacuated and refilled with hydrogen (3×), and the reaction mixture was stirred vigorously under a balloon of hydrogen for 5 h. The mixture was then filtered through celite, washing with MeOH (5 mL) and the filtrate was concentrated in vacuo to afford 24 mg (99%) of the title compound (29).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06812240B1 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-311443d9300a4918b8555750a0cdcdb2 |
| Source note | uspto-grants-2004_11 |