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HRID2414316

反应详情

EQUATION

反应方程式

HRID 2414316 的结构方程式

REACTANTS

反应物

2
结构：CC(C)N
HCID6363

Isopropylamine

C3H9N

结构：O=[N+]([O-])c1cc(S(=O)(=O)Cl)ccc1Cl
HCID7323

Benzenesulfonyl chloride, 4-chloro-3-nitro-

C6H3Cl2NO4S

PRODUCTS

生成物

1
结构：CC(C)NS(=O)(=O)c1ccc(Cl)c([N+](=O)[O-])c1
HCID66780

Benzenesulfonamide, 4-chloro-N-(1-methylethyl)-3-nitro-

C9H11ClN2O4S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

4-Chloro-3-nitrobenzenesulfonyl chloride (2 g) and isopropylamine (2.1 ml) in dichloromethane (30 ml) was stirred at room temperature for 2 h. The mixture was washed with water, 2M hydrochloric acid, water, dried and evaporated under reduced pressure. Yield 2.2 g.

WORKUP

后处理

  1. washThe mixture was washed with water, 2M hydrochloric acid, water
  2. customdried
  3. customevaporated under reduced pressure