HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 12074648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | O-[(Ethoxycarbonyl)cyanomethylenamino]-N,N,N',N'-tetramethyluronium tetrafluoroborate | HCID 2733286 | — |
| Reactant | HCID 22645713 | HCID 22645713 | — |
| Product | HCID 12074648 | HCID 12074648 | — |
Reaction Steps
100 mg (0.28 mmol) of 4-chloro-3-[3-(2-chlorobenzoyl)ureido]benzoic acid, 93 mg (0.28 mmol) of TOTU and 37 mg (0.28 mmol) of diisopropylethylamine were coupled in 1 ml of dimethylformamide. The reaction solution was washed once each with 5% strength sodium bicarbonate solution and 10% strength citric acid solution, and the organic phase was dried and concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06812250B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-1d15ad64f7924dc19e6721290649e754 |
| Source note | uspto-grants-2004_11 |