HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl bromide → HCID 22644688, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl bromide | HCID 7842 | — |
| Reactant | HCID 54394859 | HCID 54394859 | — |
| Product | HCID 22644688 | HCID 22644688 | 99.9% |
Reaction Steps
According to the procedure of Example 5, 0.800 g (2.36 mmol) of 2-(4-but-2-ynyloxy-benzenesulfonylamino)-3-methyl-butyric acid methyl ester and 0.53 g (4.72 mmol) of 80% propargyl bromide gave 0.89 g of methyl 2-[{[4-(2-butynyloxy)phenyl]sulfonyl}(2-propynyl)amino]-3-methylbutanoate as a colorless oil. Electrospray Mass Spec 378.2 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06812227B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-6884846f2a2149eb83829196d04a92bb |
| Source note | uspto-grants-2004_11 |