HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → HCID 21304716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 57134211 | HCID 57134211 | — |
| Product | HCID 21304716 | HCID 21304716 | 79.1% |
Reaction Steps
According to the procedure of Example 250, lithium iodide mediated ester cleavage of 0.282 g (0.61 mmol) of methyl (3S)-2,2-dimethyl-4-({4-[(3-phenyl-2-propynyl)oxy]phenyl}sulfonyl)-3-thiomorpholinecarboxylate provided 0.215 g (79%) of (3S)-2,2-dimethyl-4-({4-[(3-phenyl-2-propynyl)oxy]phenyl}sulfonyl)-3-thiomorpholine carboxylic acid as a white solid. Electrospray Mass Spec: 446.0 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06812227B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-f967b5ae703c433fb5ea58d538bac13f |
| Source note | uspto-grants-2004_11 |