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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2414671Generated: November 1, 2026

Lithium iodide → HCID 57142506, compound

https://huagongshe.com/reaction/2414671

Reaction equation

Participants

RoleNameHCIDCharge
ReactantLithium iodideHCID 66321—
ReactantHCID 57254020HCID 57254020—
ProductHCID 57142506HCID 57142506100.1%

Reaction Steps

According to the procedure of Example 251, lithium iodide mediated ester cleavage of 0.456 g (0.845 mmol) of tert-butyl (3S)-4-[(4-{[7-(acetyloxy)-2-heptynyl]-oxy}phenyl)sulfonyl]-2,2-dimethyl-3-thiomorpholinecarboxylate provided 0.409 g (100%) of (3S)-4-[(4-{[7-(acetyloxy)-2-heptynyl]oxy}phenyl)sulfonyl]-2,2-dimethyl-3-thiomorpholinecarboxylic acid as a colorless oil. Electrospray Mass Spec: 446.0 (M+H)+

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06812227B2
Source datasetuspto-grants-2004_11
ORD IDord-7c88fde3bf754f31b2e1daac6357f046
Source noteuspto-grants-2004_11