Methanol, 1,1-diethoxy-, 1-acetate → HCID 54000877, compound

HRID 2414744Notes

Reaction equation

HRID 2414744 reaction equation
[S:1]1[CH:5]=[CH:4][C:3]([C:6]2[CH:7]=[C:8]3[CH2:14][C:13](=[O:15])[NH:12][C:9]3=[N:10][CH:11]=2)=[CH:2]1.[C:16]([O:19][CH:20](OCC)OCC)(=O)[CH3:17]>>[CH2:16]([O:19][CH:20]=[C:14]1[C:8]2[C:9](=[N:10][CH:11]=[C:6]([C:3]3[CH:4]=[CH:5][S:1][CH:2]=3)[CH:7]=2)[NH:12][C:13]1=[O:15])[CH3:17]

Participants

3

Reactant 2

HCID 84166Methanol, 1,1-diethoxy-, 1-acetateHCID 15504071HCID 15504071, compound

Product 1

HCID 54000877HCID 54000877, compound

Procedure

This compound was synthesized from 5-(3-thienyl)-1H-pyrrolo[2,3-b]pyridin-2-one and diethoxymethyl acetate according to Procedure A. 1H NMR 400 MHz (DMSO-d6): δ 10.89 (s, 1H); 8.33 (s, 1H); 7.88 (s, 1H); 7.84 (s, 1H); 7.79 (s, 1H); 7.62 (m, 1H); 7.49 (d, 1H); 4.40 (m, 2H); 1.36 (m, 3H).

Sources & evidence

ORD record
ord-825b9c725538484cb8758463173160ef
Source dataset
uspto-grants-2004_11
Patent number
US06815439B2

Reaction notes

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