HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenylhydrazine hydrochloride → HCID 178517005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenylhydrazine hydrochloride | HCID 12157 | — |
| Reactant | 6H-thiazolo[5,4-e]indole-7,8-dione | HCID 11745756 | — |
| Product | HCID 178517005 | HCID 178517005 | 62% |
Reaction Steps
Prepared according to Example 96 with 6H-1-thia-3,6-diaza-as-indacen-7,8-dione (Procedure A) and 4-bromophenylhydrazine hydrochloride in 62% yield. 1H NMR (DMSO-d6): δ7.16 (d, J=8.5 Hz, 1H); 7.50 and 7.62 (Abq, J=8.8 Hz, 4H); 8.02 (d, J=8.5 Hz, 1H); 9.33 (s, 1H); 11.3 (s, 1H); 12.6 (s, 1H). ES-MS m/z 371, 373 (M−1)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818632B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-1054a85ad9c14f92b4e70071a222db0e |
| Source note | uspto-grants-2004_11 |