HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzylamine → HCID 12529950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzylamine | HCID 66035 | — |
| Reactant | Pyrylium, 2,4,6-triphenyl-, tetrafluoroborate(1-) | HCID 9930615 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 12529950 | HCID 12529950 | 84.1% |
Reaction Steps
A solution of 2,4,6-triphenylpyrylium tetrafluoroborate (2.97 g, 7.5 mmol) in ethanol (15 mL) was treated with 4-methylbenzylamine (1 g, 8.25 mmol). The reaction was stirred overnight at room temperature and diluted with diethyl ether to precipitate the product. The product was recrystallized from ethanol/diethyl ether to give 3.15 g of N-(4-methylbenzyl)-2,4,6-triphenylpyridinium tetrafluoroborate as a tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818660B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-cc63ac9feabf4723b7c555c3d493fd35 |
| Source note | uspto-grants-2004_11 |