HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Methoxyphenyl)-1,1-dimethylethylamine → HCID 22640965, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Methoxyphenyl)-1,1-dimethylethylamine | HCID 91892 | — |
| Reactant | 2-{[(4-Chloronaphthalen-1-yl)oxy]methyl}oxirane | HCID 5743542 | — |
| Product | HCID 22640965 | HCID 22640965 | 43.4% |
Reaction Steps
Using the method of Example 5, supra, 1,2-epoxy-3-[4-chloro-(1-naphthoxy)]propane (469 mg, 2 mmol) and 1,1-dimethyl-2-(4-methoxyphenyl)ethylamine (120 mg, 0.67 mmol) yielded, after preparative TLC and RP-HPLC, 131 mg of the title compound as a white solid: GC/EI-MS, m/z (rel. int.) 414 (M+, 0.5), 398 (1), 292 (100), 121 (33), 71 (43).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818660B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-0c953bf5af3148e0a0d451cae435cac9 |
| Source note | uspto-grants-2004_11 |