HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Methoxyphenyl)-1,1-dimethylethylamine → HCID 69471853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Methoxyphenyl)-1,1-dimethylethylamine | HCID 91892 | — |
| Reactant | HCID 15016375 | HCID 15016375 | — |
| Product | HCID 69471853 | HCID 69471853 | 103.6% |
Reaction Steps
Using the method of Example 6, supra, (S)-2,3-dichlorophenyl glycidyl ether (0.84 g, 3.82 mmol) and 1,1-dimethyl-2-(4-methoxyphenyl)ethylamine (0.75 g, 4.18 mmol) were used to prepare 860 mg of the title compound as a white solid: GC/EI-MS, m/z, (rel. int.) 382 (M−15, 0.1), 280 (10), 279 (9), 278 (63), 276 (100), 163 (11), 121 (28), 77 (7), 71 (21), 70 (23), 58 (10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818660B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-c1fa2948451c4c3cb57c1d0ca03b20e4 |
| Source note | uspto-grants-2004_11 |