HRID2415530

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)CC(CNC(=O)OC(C)OC(=O)C(C)C)CC(=O)O

HCID16059234

未命名化合物

结构：CC(C)C(=O)OC(C)c1cccc(OC(=O)[O-])c1[N+](=O)[O-]

HCID86589559

未命名化合物

PRODUCTS

生成物

结构：CC(C)CC(CNC(=O)OC(OC(=O)C(C)C)C(C)C)CC(=O)O

HCID22272016

未命名化合物

收率 51%

PROCEDURE

实验过程

Following the procedure of preparation for (110), and substituting (114) for (111), provided the title compound as a mixture of two diastereomers in 51% yield. 1H-NMR (CDCl3, 400 MHz): δ 0.89 (m, 12H), 1.17 (m, 8H), 1.65 (m, 1H), 2.02 (m, 1H), 2.16 (m, 1H), 2.33 (m, 2H), 2.56 (m, 1H), 3.13 (m, 1H), 3.30 (m, 1H), 5.00 (m, 1H), 6.57-6.56 (m, 1H).