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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 241574Generated: October 30, 2026

Trifluoroacetic acid → HCID 25196368, compound

https://huagongshe.com/reaction/241574

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 86657491HCID 86657491—
SolventDichloromethaneHCID 6344—
ProductHCID 25196368HCID 25196368—

Reaction Steps

The product from Step E was treated with 2 ml, TFA in CH2Cl2 (2 mL) for 1 h. 1H NMR (500 MHz, CD3OD): δ 7.68 (br, 1H); 7.50 (m, 6H); 7.30 (m, 2H); 7.12 (br, 1H); 4.71 (br, 4H); 3.91 (br, 2H); 3.87 (br, 2H); 3.80 (br, 1H); 3.41 (br, 1H); 3.31 (br, 1H); 3.22 (br, 1H); 2.52 (m, 1H); 2.31 (m, 1H); LC-MS: 410.08 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08653059B2
Source datasetuspto-grants-2014_02
ORD IDord-78f78448d9f0468bbc76447fcdabc344
Source noteuspto-grants-2014_02