HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 25196368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86657491 | HCID 86657491 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 25196368 | HCID 25196368 | — |
Reaction Steps
The product from Step E was treated with 2 ml, TFA in CH2Cl2 (2 mL) for 1 h. 1H NMR (500 MHz, CD3OD): δ 7.68 (br, 1H); 7.50 (m, 6H); 7.30 (m, 2H); 7.12 (br, 1H); 4.71 (br, 4H); 3.91 (br, 2H); 3.87 (br, 2H); 3.80 (br, 1H); 3.41 (br, 1H); 3.31 (br, 1H); 3.22 (br, 1H); 2.52 (m, 1H); 2.31 (m, 1H); LC-MS: 410.08 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08653059B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-78f78448d9f0468bbc76447fcdabc344 |
| Source note | uspto-grants-2014_02 |