HRID241597

反应详情

EQUATION

反应方程式

HRID 241597 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 3-nitro-4-aminophenol (4.6 g, 30 mmol) in methanol is added 500 mg of Pd/C. A hydrogenation reaction is performed at room temperature for 2 hours and then terminated. The Pd/C is removed by filtration to obtain 4.1 g of 3-hydroxy-o-phenylenediamine, with a yield of 95%.

WORKUP

后处理

  1. customA hydrogenation reaction
  2. customterminated
  3. customThe Pd/C is removed by filtration