HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → HCID 23698633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | N-(tert-butoxycarbonyl)glycine | HCID 78288 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23698633 | HCID 23698633 | — |
Reaction Steps
To a mixture of N-(tert-butoxycarbonyl)glycine (42.0 g) in water (250 ml) was added cesium carbonate (39.1 g). The mixture was stirred at room temperature for 10 minutes. The water was removed by azeotropic distillation with toluene to give the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06821992B1 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-9c600e1f40014ca3ad42a9fefa851cf8 |
| Source note | uspto-grants-2004_11 |