1,2-Bis(4-methylphenyl)-1,2-ethanedione → HCID 5052632, compound

Participants

Reaction Steps

1.84 g (12 mmol) of 2,3-diaminonitrobenzene and 2.38 g (10 mmol) of 4,4′-dimethylbenzil were dissolved in 40 g of a 1:1 mixed solvent of acetic acid/methanol, and reaction was allowed at 80° C. for 4 hr. After the reaction was over, the solvent was removed, and the reaction product was extracted on a silica gel column.

Provenance & Evidence