HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 178427528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | HCID 178427527 | HCID 178427527 | — |
| Product | HCID 178427528 | HCID 178427528 | 95% |
Reaction Steps
2.3 g of Boc-Asp(OBzl)-DPhe-NMeVal-Arg(Pbf)-Gly-OtBu are dissolved in 23 ml of 95% formic acid for the removal of the terminal protective groups and concentrated in vacuo after 30 min. The product is triturated with ether, filtered off and dried in vacuo. H-Asp(OBzl)-DPhe-NMeVal-Arg(Pbf)-Gay-OHxHCOOH is obtained in a yield of 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06822074B1 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-5f55b56e0b8d44908f479c8eb5ac5a68 |
| Source note | uspto-grants-2004_11 |