2-Aminobenzaldehyde → HCID 86610490, compound

HRID 2416187Notes

Reaction equation

HRID 2416187 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7]2([CH2:12][C:13]([OH:15])=O)[NH:11][CH:10]=[CH:9][S:8]2)[CH:2]=1.[NH2:16][C:17]1[CH:24]=[CH:23][CH:22]=[CH:21][C:18]=1[CH:19]=[O:20]>>[CH:19]([C:18]1[CH:21]=[CH:22][CH:23]=[CH:24][C:17]=1[NH:16][C:13](=[O:15])[CH2:12][C:7]1([C:3]2[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=2)[NH:11][CH:10]=[CH:9][S:8]1)=[O:20]

Participants

3

Reactant 2

HCID 682552-AminobenzaldehydeHCID 86610491HCID 86610491, compound

Product 1

HCID 86610490HCID 86610490, compound

Procedure

This compound was prepared according to the method described in Example 1c by employing 2-(3-pyridyl)-thiazole acetic acid (Step b) and o-aminobenzaldehyde (Aldrich). Mp: 70-73° C. MS m/z: 324 (M+1). Calc'd for C17H13N3O2S: 323.07.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-fe5565d1d144487884a12fdd0b1e9aeb
Source dataset
uspto-grants-2004_11
Patent number
US06822097B1

Reaction notes

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