2-Ethylaminoethyldimethylamine → HCID 23527337, compound

HRID 2416219Notes

Reaction equation

[CH2:1]([NH:3][CH2:4][CH2:5][N:6]([CH3:8])[CH3:7])[CH3:2].[N:9]1[CH:14]=[CH:13][C:12]([C:15]2[S:16][CH:17]=[C:18]([C:20]3[C:21](=[O:33])[NH:22][C:23]4[C:28]([CH:29]=3)=[CH:27][CH:26]=[C:25]([C:30](O)=[O:31])[CH:24]=4)[N:19]=2)=[CH:11][CH:10]=1>>[CH3:7][N:6]([CH3:8])[CH2:5][CH2:4][N:3]([CH2:1][CH3:2])[C:30]([C:25]1[CH:24]=[C:23]2[C:28]([CH:29]=[C:20]([C:18]3[N:19]=[C:15]([C:12]4[CH:11]=[CH:10][N:9]=[CH:14][CH:13]=4)[S:16][CH:17]=3)[C:21](=[O:33])[NH:22]2)=[CH:27][CH:26]=1)=[O:31]

Participants

Reactant 2

HCID 671622-Ethylaminoethyldimethylamine

HCID 22638545HCID 22638545, compound

Product 1

HCID 23527337HCID 23527337, compound

Procedure

This compound was prepared according to the method described in Example 8734 employing N′-ethyl-N,N-dimethylethane-1,2-diamine (Aldrich) and 3-(2-pyridin-4-yl-thiazol-4-yl)-1H-quinolin-2-one-7-carboxylic acid. MS m/z: 448.2 (M+1). Anal. Calc'd for C24H25N5O2S.1.7H2O: C, 60.28; H, 5.99; N, 14.65. Found: C, 60.03; H, 5.61; N, 14.39.

Workup

customThis compound was prepared

Sources & evidence

ORD record: ord-e46d707dc39443ff931ce87235301587
Source dataset: uspto-grants-2004_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06822097B1

Reaction notes

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