HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4-bromo-2-methylphenyl)-2,2,2-trifluoroacetamide → HCID 86759563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4-bromo-2-methylphenyl)-2,2,2-trifluoroacetamide | HCID 789606 | — |
| Reactant | HCID 17937271 | HCID 17937271 | — |
| Product | HCID 86759563 | HCID 86759563 | 66% |
Reaction Steps
Starting from 191 mg (0.68 mmol) N-(4-bromo-2-methyl-phenyl)-2,2,2-trifluoro-acetamide and 173 mg (0.34 mmol) 2-methyl-propane-1-sulphonic acid 5-(2,4-diamino-pyrimidin-5-ylmethyl)-3-ethoxy-2-iodo-phenyl ester, 109 mg of the title compound are obtained as a brown solid after chromatography and stirring in 5 ml ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06821980B1 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-25f85c69e7344363a972a6f8f66a2b5e |
| Source note | uspto-grants-2004_11 |