HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → Phenyltripropoxysilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Tetraethoxysilane | HCID 6517 | — |
| Reactant | Phenyltriethoxysilane | HCID 13075 | — |
| Solvent | Water | HCID 962 | — |
| Product | Phenyltripropoxysilane | HCID 15909578 | — |
Reaction Steps
In a 1-liter flask 297 grams (4.798 moles) 2-propanol, 148 grams (2.558 moles) acetone, 93 grams (0.448 moles) TEOS, 37 grams (0.209 moles) MTEOS, 100 grams (0.418 moles) phenyltriethoxysilane, 0.6 grams 0.1 M nitric acid and 72 grams (3.716 moles) deionized water were combined. The flask was refluxed for 4 hours. To the solution, 57 grams (0.769 moles) of Butanol, 88 grams (1.422 moles) 2-propanol, 44 grams (0.758 moles) of acetone, 59 grams (1.227 moles) of ethanol, 9.5 grams (0.528 moles) deionized water were added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06824879B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-b7b9aa6e6a194aa4903f7863196ef71c |
| Source note | uspto-grants-2004_11 |