HRID2416575

反应详情

EQUATION

反应方程式

HRID 2416575 的结构方程式

PROCEDURE

实验过程

847 mg (2.43 mmol) of ethyl (1-t-butoxycarbonyl-4-piperidyloxy)benzoate was dissolved in 50 ml of ethanol. 5 ml of 1 N sodium hydroxide solution was added to the obtained solution, and they were stirred at room temperature for 3 days. The reaction solution was concentrated and then treated with ethyl acetate as the extraction solvent in an ordinary manner to obtain the title compound.

WORKUP

后处理

  1. concentrationThe reaction solution was concentrated
  2. additiontreated with ethyl acetate as the extraction solvent in an ordinary manner