HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22632917, compound → HCID 22632945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22632917 | HCID 22632917 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 22632945 | HCID 22632945 | 118.8% |
Reaction Steps
Using the General Method 6A, the reaction of 10% Pd/C (0.03 g) with 1-(4-methoxyphenyl)-6-fluoro-3-benzyloxy-7-pyrrolidin-1-yl-1H-quinazoline-2,4-dione (Example O-1, 0.09 g, 0.195 mmol) afforded 0.086 g of the title compound as a solid, mp 224-226° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825199B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-e35da75a8d75467fa6c90d1d37119799 |
| Source note | uspto-grants-2004_11 |