HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2416982Generated: October 31, 2026
Triethyl phosphite → HCID 22630521, compound
https://huagongshe.com/reaction/2416982
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | HCID 22630504 | HCID 22630504 | — |
| Product | HCID 22630521 | HCID 22630521 | 101.7% |
Reaction Steps
A mixture of 0.98 g of 1-bromo-22-(nonafluorobutyl)docosane and 4.00 g of triethyl phosphite was heated at 150° C. After 18 hr, diethyl ethylphosphonate and other volatiles were distilled, b.p. 30-50° C. at 0.05 torr (7 Pa), leaving 1.09 g of 1-(diethylphosphono)-22-(nonafluorobutyl)docosane as an off-white solid, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06824882B2 |
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| Source dataset | uspto-grants-2004_11 |
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| ORD ID | ord-6a1a806c5278465588dc47cf1e7efede |
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| Source note | uspto-grants-2004_11 |
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