Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | Hexamethylene diisocyanate | HCID 13192 | — |
| Reactant | 1,3-Bis(isocyanatomethyl)benzene | HCID 19262 | — |
| Reactant | Di-n-butyldilauryltin | HCID 9809426 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Urethane acrylate | HCID 21863578 | — |
Reaction Steps
Into a flask similar to the flask in Synthesis Example 1 were charged 50 parts of toluene, 50 parts of hexamethylene diisocyanate subjected to isocyanurate modification (TAKENATE D-170N), 94 parts of polycaprolactone-modified hydroxyethyl acrylate (PLACCEL FA2D), 0.02 parts of dibutyltin laurate, and 0.02 parts of hydroquinone monomethyl ether. The mixture was maintained at 70° C. for 5 hours to complete the reaction, and 94 parts of toluene were added to obtain a urethane acrylate containing 50% by weight of solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06825243B2 |
|---|
| Source dataset | uspto-grants-2004_11 |
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| ORD ID | ord-0d49dc0f237c433fba9bf12a55b09c3b |
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| Source note | uspto-grants-2004_11 |
|---|
