HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-((Benzyloxy)carbonyl)-2-methylalanine → HCID 131724668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-((Benzyloxy)carbonyl)-2-methylalanine | HCID 294936 | — |
| Reactant | HCID 58726315 | HCID 58726315 | — |
| Product | HCID 131724668 | HCID 131724668 | 85.4% |
Reaction Steps
H-L-Phe-D-Pro-OtBu (0.853 g, 2.68 mmol) and Z-Aib-OH (954 mg, 4.02 mmol) were condensed as described in Step 1 above. The oily product was purified by flash chromatography on silica gel (CHCl3/MeOH=99/1) to yield 1.23 g (85%) of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825317B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-5c9e1fecf77f4755bcd79a32343d256b |
| Source note | uspto-grants-2004_11 |