1-Bromo-2-butyne → HCID 11337003, compound

Participants

Reaction Steps

2-(4-But-2-ynyloxy-phenylsulfanyl)-octanoic acid ethyl ester was prepared according to the general method as outlined in Example 1 (Step 2). Starting from 2-(4-hydroxy-phenylsulfanyl)-octanoic acid ethyl ester 13.6 g, 46 mmol) and 1-bromo-2-butyne (6.23 g, 47 mmol). Yield 13.78 g (86%); amber oil; MS: 349.0 (M+H)+

Provenance & Evidence