HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22340599, compound → 4-(4-Hydroxy-phenoxy)-butyric acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22340599 | HCID 22340599 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(4-Hydroxy-phenoxy)-butyric acid ethyl ester | HCID 18918590 | 79.9% |
Reaction Steps
To a solution of 3.58 g (0.011 mol) of 4-(4-Benzyloxy-phenoxy)-butyric acid ethyl ester in 200 mL of ethanol was added 0.81 g of 5% palladium on carbon and the resulting mixture was shaken under 35 psi of hydrogen for 4 h. The resulting mixture was filtered through Magnesol® and concentrated in vacuo to provide 1.97 g of the phenol as a grey solid. Electrospray Mass Spec: 225 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825354B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-ea8c4640b3c04a69919ff7b74c4f8cce |
| Source note | uspto-grants-2004_11 |