HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-bromo-2-(4-chlorophenyl)acetate → Ethyl(4-chlorophenyl)[(4-hydroxyphenyl)sulfanyl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-bromo-2-(4-chlorophenyl)acetate | HCID 228840 | — |
| Reactant | 4-Mercaptophenol | HCID 240147 | — |
| Product | Ethyl(4-chlorophenyl)[(4-hydroxyphenyl)sulfanyl]acetate | HCID 91432097 | 97% |
Reaction Steps
Ethyl(4-chlorophenyl)[(4-hydroxyphenyl)sulfanyl]acetate was prepared according to the general method as outlined in example 1 (step 1), starting from ethyl bromo(4-chlorophenyl)acetate (16.5 g, 59.6 mmol) and 4-mercaptophenol (7.5 g, 59.6 mmol); 18.8 g white solid. mp: 63° C.; Yield 97%; MS: 321.3 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825354B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-66f87649ff7a4385a98b78b68f10c182 |
| Source note | uspto-grants-2004_11 |