HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Mercaptophenol → Ethyl(4-bromophenyl)[(4-hydroxyphenyl)sulfanyl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Mercaptophenol | HCID 240147 | — |
| Reactant | Ethyl 2-bromo-(4-bromophenyl)acetate | HCID 12754876 | — |
| Product | Ethyl(4-bromophenyl)[(4-hydroxyphenyl)sulfanyl]acetate | HCID 91031423 | 92% |
Reaction Steps
Ethyl(4-bromophenyl)[(4-hydroxyphenyl)sulfanyl]acetate was prepared according to the general method as outlined in example 1 (step 1), starting from ethyl bromo(4-bromophenyl)acetate (15 g, 45.6 mmol) and 4-mercaptophenol (5.75 g, 45.6 mmol); 15.39 g white solid. mp: 55.6° C.; Yield 92%; MS: 365.1 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825354B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-0f5a2601cacd49a390f5b5020ccab32d |
| Source note | uspto-grants-2004_11 |