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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2417461Generated: October 31, 2026

Trifluoroacetic acid → HCID 69892979, compound

https://huagongshe.com/reaction/2417461

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 86589870HCID 86589870—
SolventDichloromethaneHCID 6344—
ProductHCID 69892979HCID 69892979—

Reaction Steps

400 mg (0.97 mmol) of t-butyl [4-(4-chlorobenzoyl)-2-oxo-2,3,4,5-tetrahydrobenzo[e][1,4]diazepin-1-yl]acetate was dissolved in a mixture of 2 ml of dichloromethane and 2 ml of trifluoroacetic acid, and the obtained solution was stirred at room temperature for 1 hour. The solvent was evaporated to obtain the crude title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06825191B2
Source datasetuspto-grants-2004_11
ORD IDord-e0c7f1ac54244cbab4822c886f82a94f
Source noteuspto-grants-2004_11