HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 69892979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86589870 | HCID 86589870 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69892979 | HCID 69892979 | — |
Reaction Steps
400 mg (0.97 mmol) of t-butyl [4-(4-chlorobenzoyl)-2-oxo-2,3,4,5-tetrahydrobenzo[e][1,4]diazepin-1-yl]acetate was dissolved in a mixture of 2 ml of dichloromethane and 2 ml of trifluoroacetic acid, and the obtained solution was stirred at room temperature for 1 hour. The solvent was evaporated to obtain the crude title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825191B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-e0c7f1ac54244cbab4822c886f82a94f |
| Source note | uspto-grants-2004_11 |