Triethylamine → HCID 86589874, compound

Participants

Reaction Conditions

Reaction Steps

580 mg (1.27 mmol) of ethyl [(2-nitro-4-bromobenzyl)-(4-chlorobenzoyl)amino]acetate, 28 mg (0.13 mmol) of palladium acetate, 0.23 ml (1.6 mmol) of diethylvinyl phosphonate, 233 mg (0.89 mmol) of triphenylphosphine and 0.35 ml (2.5 mmol) of triethylamine were dissolved in 10 ml of DMF. They were stirred at 100° C. for 4 hours. After the treatment with ethyl acetate as the extracting solvent by an ordinary method, the crude product was obtained. The crude product was purified by the silica gel column chromatography to obtain the title compound.

Provenance & Evidence