Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 1-(1H-Imidazol-1-yl)ethanone | HCID 17174 | — |
| Reactant | Ethyl 4-(3-bromoprop-1-en-1-yl)benzoate | HCID 54306695 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178468846 | HCID 178468846 | 95.3% |
Reaction Steps
To 10 ml of dry acetonitrile were added 3.3 g of 1-acetylimidazole and 8.04 g of 4-ethoxycarbonylcinnamyl bromide, and the mixture was heated for 3 hours at 60° C. under stirring. After cooling, to the reaction mixture was added an adequate amount of dry diethyl ether and the resulting powder was collected by filtration and dried to obtain 10.8 g of 1-acetyl-3-(4-ethoxycarbonylcinnamyl)-imidazolium bromide. (colorless hygroscopic amorphous).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04469865 |
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| Source dataset | uspto-grants-1984_09 |
|---|
| ORD ID | ord-9d9a533092cc4c78b025e15141364be4 |
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| Source note | uspto-grants-1984_09 |
|---|
