Sodium Iodide → HCID 13338392, compound

Participants

Reaction Steps

The above aziridine (12 g, 0.05 mol) is dissolved in 100 ml of acetone and refluxed with 10 g of sodium iodide for 2.5 hours. The mixture is evaporated in vacuo. The residue is dissolved in methylene dichloride and washed with a saturated solution of NaHCO3. The organic solution is dried (MgSO4) and evaporated in vacuo. The residual oil is crystallized from ethyl acetate ether to give 3.1 g (30%) of title compound, mp 107°-110° C.

Provenance & Evidence