HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 13338394, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 7-(Aziridin-1-yl)-1-ethyl-3,5-dimethyl-1H-pyrazolo[4,3-d]pyrimidine | HCID 13338433 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 13338394 | HCID 13338394 | 57% |
Reaction Steps
The above aziridine (14 g, 0.065 mol) is dissolved in 150 ml acetone and 12 g (0.08 mol) of sodium iodide is added. The mixture is stirred overnight as a solid separates. The cooled mixture is filtered, the filter cake is washed with saturated NaHCO3 solution then water to yield 8 g (57%) of the title compound, mp 168°-170° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04469868 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-c358f2298b774c6ea15b5b92d7b141c3 |
| Source note | uspto-grants-1984_09 |