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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2417684Generated: November 2, 2026

Hydrogen Peroxide → HCID 178456656, compound

https://huagongshe.com/reaction/2417684

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen PeroxideHCID 784—
ReactantWaterHCID 962—
ReactantSodium HydroxideHCID 14798—
ReactantN-(5-Cyano-3-methyl-1-propyl-1H-pyrazol-4-yl)acetamideHCID 13338440—
SolventAcetic AcidHCID 176—
ProductHCID 178456656HCID 17845665666%

Reaction Conditions

Temperature80 °C

Reaction Steps

The above acetamide (16 g, 0.085 mol) is added in portions with stirring at 80° C. to a solution prepared by adding 24 ml of 30% hydrogen peroxide to 200 ml water containing 6 g (0.015 mol) of sodium hydroxide. After stirring at 80° C. for five hours, the mixture is cooled, acidified with acetic acid, and filtered to give 11.6 g (66%) of the title compound, mp 196°-198° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04469868
Source datasetuspto-grants-1984_09
ORD IDord-23dff3078bfa4139918a573a755e386e
Source noteuspto-grants-1984_09