Calcium Carbonate → HCID 14774580, compound

HRID 2417755Notes

Reaction equation

HRID 2417755 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([C:8]([CH3:12])=[CH:9][C:10]=1[NH2:11])[NH2:7])([O-:3])=[O:2].C(=O)([O-])[O-].[Ca+2].Cl[CH2:19][CH2:20][CH2:21][OH:22]>O>[N+:1]([C:4]1[CH:5]=[C:6]([C:8]([CH3:12])=[CH:9][C:10]=1[NH2:11])[NH:7][CH2:19][CH2:20][CH2:21][OH:22])([O-:3])=[O:2]

Participants

5

Reactant 3

HCID 10112Calcium CarbonateHCID 123133-Chloro-1-propanolHCID 54879441,4-Benzenediamine, 2-methyl-5-nitro-

Product 1

HCID 14774580HCID 14774580, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

16.7 g (0.1 mol) of 3-nitro-4-amino-6-methylaniline, 40 ml of water, 6.6 g (0.066 mol) of calcium carbonate and 12.42 g (0.132 mol) of 3-chloropropan-1-ol are heated on a boiling water-bath for 7 hours 30 minutes, whilst stirring.

Sources & evidence

ORD record
ord-d44983e8aad846a2bb757d403a9e1103
Source dataset
uspto-grants-1984_09
Patent number
US04470826

Reaction notes

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