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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2417758Erstellt: 25. Oktober 2026

Chlorine → 1-Chloro-4-(trifluoromethoxy)benzene

https://huagongshe.com/reaction/2417758

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktChlorineHCID 24526—
Edukt1-Nitro-4-(trifluoromethoxy)benzeneHCID 522405—
Produkt1-Chloro-4-(trifluoromethoxy)benzeneHCID 277727383%

Reaktionsschritte

Chlorine and p-nitrotrifluoromethoxybenzene (10.7 parts) were fed simultaneously at a molar ratio of 3:1, Cl2 :organic reactant, into a vapor phase reactor maintained at 300° C. to 320° C. over a 30 minute period to yield 8.2 parts of p-chlorotrifluoromethoxybenzene (83% yield). The structure of the product was confirmed by gas chromatographic--mass spectrum and F19 nuclear magnetic resonance analysis.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04470930
Quelldatensatzuspto-grants-1984_09
ORD IDord-665b3233577e40e2b738511d049dd05c
Quellennotizuspto-grants-1984_09