HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 20446686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 20446656 | HCID 20446656 | — |
| Product | HCID 20446686 | HCID 20446686 | — |
Reaction Steps
2-Aminomethyl-4-(3-methoxycarbonylpropyl)pyridine (0.11 g) is heated at 90° in 0.5 ml of 97% formic acid for 18 hours. The reaction is cooled to room temperature, made basic with ammonium hydroxide solution and extracted with methylene chloride (4×20 ml). The organic extracts are dried over sodium sulfate and evaporated to yield 2-(N-formylaminomethyl)-4-(3-methoxycarbonylpropyl)pyridine; IR (CH2Cl2) 1735, 1685 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04470986 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-e2281b38fe2f46cea61946f26a5171af |
| Source note | uspto-grants-1984_09 |