Triethylamine → HCID 54085480, compound

Participants

Reaction Steps

A mixture comprising 2.6 g of 4-methoxyphenyl 2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside in 25 ml of cold methanol was combined with a cold mixture of 2N triethylamine in methanol:water (6:2). This mixture was refrigerated overnight, then evaporated in vacuo to a solid which was triturated with ether, giving 1.3 g of the desired intermediate, UV 225-245 nm.

Provenance & Evidence