HuagongsheHuagongshe Chemistry Print Report · For research reference only
Monobenzone → 1-(Benzyloxy)-4-[(5-bromopentyl)oxy]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Monobenzone | HCID 7638 | — |
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1-(Benzyloxy)-4-[(5-bromopentyl)oxy]benzene | HCID 13219124 | — |
Reaction Steps
4-Benzyloxyphenol and 1,5-dibromopentane were reacted under conditions described in Example 15 for 5 days. The crude product isolated by a toluene extraction, was distilled to give 1-benzyloxy-4-(5-bromopentoxy)benzene as an oil (88.9% pure by gas chromatography).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04471116 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-d36770889b2043d3b5dee7a413e1dbba |
| Source note | uspto-grants-1984_09 |