HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 1-Benzyloxy-4-(3-dimethylaminopropoxy)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 1-Benzyloxy-4-(3-methylaminopropoxy)benzene | HCID 2199120 | — |
| Reactant | 1-(Benzyloxy)-4-(3-bromopropoxy)benzene | HCID 11110031 | — |
| Product | 1-Benzyloxy-4-(3-dimethylaminopropoxy)benzene | HCID 2480942 | — |
Reaction Steps
In the manner described above for the preparation of 1-benzyloxy-4-(3-methylaminopropoxy)benzene, 1-benzyloxy-4-(3-bromopropyloxy)benzene was reacted with dimethylamine to give 1-benzyloxy-4-(3-dimethylaminopropoxy)benzene. The product was isolated as its hydrochloride salt and crystallization from isopropanol gave the purified hydrochloride salt of 1-benzyloxy-4-(3-dimethylaminopropoxy)benzene, mp 183°-185°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04471116 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-8243a2bd56144ca5a420b0f4d5bf4b73 |
| Source note | uspto-grants-1984_09 |