HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178482529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 3,4-Dimethoxy-1,2,5-thiadiazole 1,1-dioxide | HCID 12230538 | — |
| Reactant | HCID 12943529 | HCID 12943529 | — |
| Reactant | HCID 178494338 | HCID 178494338 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178482529 | HCID 178482529 | — |
Reaction Steps
When a methanol suspension of 3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide is reacted with an equimolar amount of 2-[(5-dimethylaminomethyl-3-methyl-2-furyl)methylthio]ethylamine [prepared in Step B] and the resultant 3-{2-[(5-dimethylaminomethyl-3-methyl-2-furyl)methylthio]ethylamino}-4-methoxy-1,2,5-thiadiazole 1,1-dioxide is treated with an excess of methylamine, the title compound is thereby produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04471122 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-a937e694242d47d8a212a4f9fad3c6f2 |
| Source note | uspto-grants-1984_09 |