HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → 3-N-[2-[[5-[(dimethylamino)methyl]furan-2-yl]methylsulfanyl]ethyl]-4-N-ethyl-1,1-dioxo-1,2,5-thiadiazole-3,4-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 5-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamine | HCID 162203 | — |
| Reactant | 3,4-Dimethoxy-1,2,5-thiadiazole 1,1-dioxide | HCID 12230538 | — |
| Reactant | N-ethyl-4-methoxy-1,1-dioxo-1,2,5-thiadiazol-3-amine | HCID 178463655 | — |
| Product | 3-N-[2-[[5-[(dimethylamino)methyl]furan-2-yl]methylsulfanyl]ethyl]-4-N-ethyl-1,1-dioxo-1,2,5-thiadiazole-3,4-diamine | HCID 178463654 | — |
Reaction Steps
Reaction of a methanolic suspension of 3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide with one equivalent of ethylamine and treatment of the resultant 3-methoxy-4-ethylamino-1,2,5-thiadiazole 1,1-dioxide with one equivalent of 2-[(5-dimethylaminomethyl-2-furyl)methylthio]ethylamine yields the title compound, which is identical to the product prepared in Example 12.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04471122 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-8a1cf8c9f9e6495f962b0ae4a8df1d00 |
| Source note | uspto-grants-1984_09 |