HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinemethanamine → 3-Methoxy-4-(3-pyridyl)methylamino-1,2,5-thiadiazole 1-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinemethanamine | HCID 31018 | — |
| Reactant | 3,4-Dimethoxy-1,2,5-thiadiazole 1-oxide | HCID 12913947 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Methoxy-4-(3-pyridyl)methylamino-1,2,5-thiadiazole 1-oxide | HCID 20402045 | — |
Reaction Steps
A solution of 3-aminomethylpyridine (2.02 g; 18.7 mmoles) in 80 ml of methanol was added dropwise over 40 minutes to a partial suspension of 3,4-dimethoxy-1,2,5-thiadiazole 1-oxide (3.03 g; 18.7 mmoles) in 150 ml of methanol, to produce a methanol solution of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04471122 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-de0e10ca3f1d4952b8971aa44b90624b |
| Source note | uspto-grants-1984_09 |