HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Ethyl 4-[4-(4-methylphenoxy)phenyl]-4-oxobut-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 4-[4-(4-Methylphenoxy)phenyl]-4-oxobut-2-enoic acid | HCID 54150157 | — |
| Reactant | HCID 54511907 | HCID 54511907 | — |
| Product | Ethyl 4-[4-(4-methylphenoxy)phenyl]-4-oxobut-2-enoate | HCID 53690715 | 76.4% |
Reaction Steps
The procedure in Example 12(1) was followed, except that 5.64 g of 3-[4-(4-methylphenoxy)benzoyl]acrylic acid and 5.98 g of ethyl iodide were used in place of 3-(4-phenoxybenzoyl)acrylic acid and methyl iodide, respectively, to give 4.74 g of ethyl 3-[4-(4-methylphenoxy)benzoyl]acrylate in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472316 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-5f82d6dc68234b8bbf3da3c426dabea8 |
| Source note | uspto-grants-1984_09 |